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Low-temperature diffusion hardening · S-Phase / expanded austenite

Hard where it wears.
Stainless where it counts.

Our NEXT-Phase™ process diffuses carbon and nitrogen into stainless steel below the temperature at which chromium carbides and nitrides can form. The surface gets up to five times harder. The corrosion resistance you specified the alloy for stays exactly where it was.

5–7 day lead time. The process is low and slow. Your turnaround is not.

Mirror-polished machined stainless steel components on a white studio surface: a ball valve body, a pump impeller, tube ferrules, a flange, a pump shaft and hex-head fasteners.

Coating-free alternative

The new coating-free alternative to tungsten carbide thermal spray coatings.

And to hard chrome plating, nickel plating, PVD/CVD coatings, boronizing, QPQ, MELONITE®/TUFFTRIDE® and Malcomizing. NEXT-Phase™ hardens the stainless itself, so there is no coating to chip, spall or corrode underneath.

NEXT-Phase™ versus tungsten carbide

Tungsten carbide thermal spray

HVOF WC-Co is typically 1050–1350 HV, sprayed 75–380 µm thick and ground to size. NEXT-Phase™ reaches comparable hardness with no layer to grind, no bond line to chip, and no line-of-sight limit in bores.

Hard chrome plating

No hexavalent chromium, no plating thickness to control and no microcrack network for corrosion to follow.

Nickel and electroless nickel

Nothing is deposited, so nothing can peel, blister or build up on edges and threads.

PVD and CVD coatings

Not line of sight and no adhesion interface. Bores, threads and internal passages harden along with the outside.

Boronizing

Boronizing runs at 700–1000 °C and ties chromium up in borides. We stay at or below 450 °C and keep it in solution.

QPQ

Salt-bath nitrocarburizing runs near 550–570 °C, where stainless forms chromium nitrides and loses its corrosion resistance.

MELONITE® and TUFFTRIDE®

The same salt-bath family. Hard, but at the cost of corrosion resistance on stainless. No molten salts are used in our process.

Malcomizing

Gas nitriding of stainless at roughly 495–565 °C (920–1050 °F), inside the chromium-nitride range. NEXT-Phase™ stays below it.

1000–1500HV0.05

Typical treated surface hardness, from a 200 HV base

≤ 450°C

Process temperature — below the chromium nitride precipitation window

10–50µm

Diffusion case depth. No coating, no interface to delaminate

±0growth

No measurable dimensional change. Tight-tolerance parts need no refinishing

The trade-off we remove

Stainless steel is specified for corrosion. It is rarely specified for wear.

Austenitic grades such as 304 and 316L are corrosion resistant because chromium in solid solution builds a passive oxide film. That same austenitic structure is soft — typically around 200 HV — it work-hardens rather than resisting wear, and it galls catastrophically when it slides against itself.

The conventional fixes both cost you something. Nitriding at 500–580 °C and carburizing at 850–950 °C precipitate chromium nitrides and carbides, pulling chromium out of solution and destroying the corrosion resistance you paid for. Hard coatings such as PVD, DLC and hard chrome introduce a mechanical interface that can chip, delaminate under load, and mask corrosion beneath it.

NEXT-Phase™ does neither. It is a diffusion treatment run cold enough that no chromium compounds can form.

A stainless steel mesh heat-treatment basket viewed from above, filled with an orderly single layer of small polished stainless steel gears, ferrules and threaded inserts.
Batch processing in mesh baskets. Because treatment is gaseous and diffusion driven, every exposed surface hardens uniformly — including bores, blind holes, threads and internal passages that a line-of-sight coating cannot reach.

What we actually create

Expanded austenite — the S-phase.

At low temperature, chromium is effectively immobile while carbon and nitrogen still diffuse freely. We exploit that gap: interstitial carbon and nitrogen are driven into the austenite lattice far past their equilibrium solubility — nitrogen contents near 28 at.% have been measured in treated 316L — and the lattice simply swells by a few percent to accommodate them.

The result is a supersaturated, precipitate-free single phase: expanded austenite, also called the S-phase. Hardness comes from extreme solid-solution strengthening combined with very high compressive residual stress. Chromium never leaves solution, so the passive film reforms exactly as before.

  • Not a coating. The hardened zone is the original part, chemically modified. There is no interface, so nothing can flake, chip or delaminate.
  • No brittle phases. The case is hard but ductile, and it deforms with the substrate instead of cracking off it.
  • Colour and finish preserved. A polished part comes back polished. Ra is essentially unchanged.
Schematic cross-section of NEXT-Phase treated AISI 316L: a nitrogen-rich S-phase layer from 0 to about 12 microns over a carbon-rich S-phase layer to about 30 microns, above an unchanged austenite substrate, with nitrogen and carbon concentration profiles against depth.
Schematic cross-section of NEXT-Phase™ treated 316L. Nitrogen concentrates in an outer, very hard γN layer; carbon diffuses ahead of it to form a deeper γC layer that supports the case. Both are expanded austenite — a diffusion zone, not a coating — and the substrate below is unchanged.

Hardness profile

A hardness gradient, not a hard shell.

Hardness falls smoothly from the surface into the bulk, which is why the case carries load without spalling. Depth is set by time and temperature, so we tune it to the application: a thin case for a polished sealing face, a deeper case for rolling and sliding contact.

Micro-hardness against depth below surface

Representative profiles for low-temperature treated austenitic stainless steel, compiled from published data. Actual values depend on alloy and treatment time.

What you gain

Six properties change. One does not.

Surface hardness

From roughly 200 HV as-supplied to 1000–1500 HV0.05 at the surface. Abrasive and adhesive wear rates drop by orders of magnitude.

Galling and seizure

The classic stainless-on-stainless failure. A treated mating pair resists cold welding, so threaded joints, valve stems and sliding fits stop seizing.

Fatigue strength

High compressive residual stress in the case suppresses surface crack initiation, raising bending and rotating fatigue limits.

Corrosion resistance — unchanged

The one property that does not move. Chromium stays in solid solution, no sensitisation occurs, and in some conditions pitting resistance measurably improves.

Dimensional stability

Case growth is at the micron scale and the process runs far below any distortion or tempering threshold. Finished, tight-tolerance parts are treated as-is.

Cavitation and erosion

Pump impellers, nozzles and valve trim last longer where high-velocity fluid and entrained solids attack the surface.

Working with us

We prove it on your part before you release production.

Every alloy, surface condition and geometry behaves slightly differently. So we do not quote from a catalogue — we run your part, section it, and show you the data.

Start a sample trial
01

Technical review

Send drawings or samples with the alloy, heat treatment condition, surface finish and the failure mode you are seeing. We confirm suitability and recommend a process route.

02

Sample trial

We treat representative parts and return them with a metallurgical report: micro-hardness traverse, case depth measurement, cross-section metallography and dimensional check.

03

Production release

Once the route is fixed, parameters are locked to a written process specification so results are repeatable batch to batch.

04

Ongoing production

Batch traceability, retained process records and periodic verification coupons run alongside your parts.

Send us a part. We will tell you what it can do.

Share a drawing, the alloy, and the failure mode you are fighting. We will recommend a process route and run a sample trial with a metallurgical report before you commit to production.